C₆₁H₁₀₀O₁₅Si₂

Base Information

Chemical Name:C₆₁H₁₀₀O₁₅Si₂
CAS No.:215876-27-0
Molecular Formula:C₆₁H₁₀₀O₁₅Si₂
Molecular Weight:1129.63
Hs Code.:

C<sub>61</sub>H<sub>100</sub>O<sub>15</sub>Si<sub>2</sub>

Synonyms:C₆₁H₁₀₀O₁₅Si₂

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Chemical Property of C₆₁H₁₀₀O₁₅Si₂

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Technology Process of C₆₁H₁₀₀O₁₅Si₂

There total 2 articles about C₆₁H₁₀₀O₁₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 215876-26-9
C₅₆H₇₈O₁₅

: 215876-27-0
C₆₁H₁₀₀O₁₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / DMAP / CH₂Cl₂ / 10 °C

2: 62 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethyl acetate

With dmap; cyclohexa-1,4-diene; palladium on activated charcoal; In dichloromethane; ethyl acetate; 1: silylation / 2: debenzylation;
DOI:10.1021/ja990860j

Reference yield:

: 215876-25-8
C₇₉H₁₃₂O₁₅Si₄

: 215876-27-0
C₆₁H₁₀₀O₁₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: HF*pyr; pyridine / tetrahydrofuran / 72 h

2: 65 percent / DMAP / CH₂Cl₂ / 10 °C

3: 62 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethyl acetate

With pyridine; dmap; cyclohexa-1,4-diene; pyridine hydrogenfluoride; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; 1: Cyclization / 2: silylation / 3: debenzylation;
DOI:10.1021/ja990860j

Reference yield:

: 215876-27-0
C₆₁H₁₀₀O₁₅Si₂

: 215876-31-6
C₅₈H₈₆O₁₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: i-PrNEt₂ / benzene

2.1: 81 percent / DMAP / benzene

3.1: PPTS; HC(OCH₃)3 / methanol; CH₂Cl₂ / -30 °C

4.1: 66 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂

5.1: NaHMDS / tetrahydrofuran / -78 °C

5.2: 75 percent / tetrahydrofuran / -15 °C

With pyridine; dmap; N,N-diethyl-N-isopropylamine; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; Dess-Martin periodane; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; benzene; 1.1: Esterification / 2.1: Cyclization / 3.1: desilylation / 4.1: Oxidation / 5.1: Metallation / 5.2: Substitution;
DOI:10.1021/ja990860j