Technology Process of C26H28O10
There total 16 articles about C26H28O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 6h;
Inert atmosphere;
Industry scale;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Industry scale
2: trifluoroacetic acid / 4 h / 20 °C / Industry scale
3: 1H-imidazole / dichloromethane / 3 h / 20 °C / Inert atmosphere; Industry scale
4: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere; Industry scale
5: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere; Industry scale
With
pyridine; 1H-imidazole; dmap; tetrabutyl ammonium fluoride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 10 - 20 °C / Inert atmosphere
2: trifluoroacetic acid / 5 °C
3: 1H-imidazole / dichloromethane / 3 h / -20 - 20 °C
4: pyridine / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere
5: 1H-imidazole; tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; tetrabutyl ammonium fluoride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
dmap;
In
tetrahydrofuran; dichloromethane;