C₄₀H₃₆O₅

Base Information

• Chemical Name: C₄₀H₃₆O₅
• CAS No.: 1354327-71-1
• Molecular Formula: C₄₀H₃₆O₅
• Molecular Weight: 596.723
• Mol file: 1354327-71-1.mol

Synonyms:C₄₀H₃₆O₅

Chemical Property of C₄₀H₃₆O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₃₆O₅

There total 4 articles about C₄₀H₃₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 6-O-trityl-3,4-di-O-benzyl-D-glucal → C40H36O5 (1354327-71-1)

Guidance literature:

With trichlorophosphate; at 0 - 20 ℃; for 13.5h; Inert atmosphere;

DOI:10.1021/ml200278u

Reference yield:

trityl chloride (76-83-5) → C40H36O5 (1354327-71-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap / pyridine / 18 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: trichlorophosphate / 13.5 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium hydride; trichlorophosphate; In pyridine; N,N-dimethyl-formamide; mineral oil; 3.1: Vilsmeier-Haack reaction;

DOI:10.1021/ml200278u

Reference yield:

D-galactal (21193-75-9) → C40H36O5 (1354327-71-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dmap / pyridine / 18 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: trichlorophosphate / 13.5 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium hydride; trichlorophosphate; In pyridine; N,N-dimethyl-formamide; mineral oil; 3.1: Vilsmeier-Haack reaction;

DOI:10.1021/ml200278u

upstream raw materials:

trityl chloride

2-((trityloxy)methyl)-3,4-dihydro-2H-pyran-3,4-diol

N,N-dimethyl-formamide

D-galactal

Downstream raw materials:

C₅₃H₅₆N₂O₄

C₅₂H₅₄N₂O₅

C₅₁H₅₉N₅O₃

C₃₂H₄₅N₅O₃