C₂₄H₂₄N₂O₃

Base Information

Chemical Name:C₂₄H₂₄N₂O₃
CAS No.:189952-83-8
Molecular Formula:C₂₄H₂₄N₂O₃
Molecular Weight:388.466
Hs Code.:

C<sub>24</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₄H₂₄N₂O₃

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Chemical Property of C₂₄H₂₄N₂O₃

Chemical Property:

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Technology Process of C₂₄H₂₄N₂O₃

There total 10 articles about C₂₄H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 189952-82-7
(1R,5S,12S)-N-benzyloxycarbonyl-12-ethyl-3-oxo-1,2,3,4,5,6-hexahydro-1,5-methanoazocino[4,3-b]indole

: 189952-83-8
C₂₄H₂₄N₂O₃

Guidance literature:: With tert.-butylhydroperoxide; dipyridinium dichromate; Celite; In benzene; Ambient temperature;
DOI:10.1039/a700856b

Reference yield:

: 189952-76-9
Benzyl-[(S)-3-(1-formyl-propyl)-hex-5-ynyl]-carbamic acid tert-butyl ester

: 189952-83-8
C₂₄H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / Me₃SiOTf / tetrahydrofuran / -78 °C

2: 86 percent / PdCl₂(PPh₃)2, CuI, Et₃N / Heating

3: 64 percent / NaOEt / ethanol / Heating

4: 54 percent / TFA / Heating

5: HCO₂NH₄ / 10percent Pd/C / methanol / Heating

6: K₂CO₃ / CH₂Cl₂

7: 54 percent / PDC/Celite, TBHP / benzene / Ambient temperature

With tert.-butylhydroperoxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; dipyridinium dichromate; trimethylsilyl trifluoromethanesulfonate; Celite; ammonium formate; sodium ethanolate; potassium carbonate; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;
DOI:10.1039/a700856b

Reference yield:

: 189952-75-8
(S)-3-[2-(Benzyl-tert-butoxycarbonyl-amino)-ethyl]-2-ethyl-hex-5-ynoic acid methyl ester

: 189952-83-8
C₂₄H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 9 steps

1: LAH / tetrahydrofuran

2: Swern oxidation

3: 83 percent / Me₃SiOTf / tetrahydrofuran / -78 °C

4: 86 percent / PdCl₂(PPh₃)2, CuI, Et₃N / Heating

5: 64 percent / NaOEt / ethanol / Heating

6: 54 percent / TFA / Heating

7: HCO₂NH₄ / 10percent Pd/C / methanol / Heating

8: K₂CO₃ / CH₂Cl₂

9: 54 percent / PDC/Celite, TBHP / benzene / Ambient temperature

With tert.-butylhydroperoxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; dipyridinium dichromate; trimethylsilyl trifluoromethanesulfonate; Celite; ammonium formate; sodium ethanolate; potassium carbonate; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;
DOI:10.1039/a700856b