α(1,2),α(1,6)-pseudomannotriose

Base Information

Chemical Name:α(1,2),α(1,6)-pseudomannotriose
CAS No.:1207538-22-4
Molecular Formula:C₂₄H₄₁NO₁₆
Molecular Weight:599.587
Hs Code.:

Synonyms:α(1,2),α(1,6)-pseudomannotriose

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Chemical Property of α(1,2),α(1,6)-pseudomannotriose

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Technology Process of α(1,2),α(1,6)-pseudomannotriose

There total 9 articles about α(1,2),α(1,6)-pseudomannotriose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1207538-17-7
C₂₄H₃₉N₃O₁₆

: 1207538-22-4
α(1,2),α(1,6)-pseudomannotriose

Guidance literature:: With palladium on carbon; hydrogen; In methanol;
DOI:10.1021/cb900216e

Reference yield:

: 140428-83-7
2-azidoethyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 1207538-22-4
α(1,2),α(1,6)-pseudomannotriose

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium methylate; methanol / 0.33 h / 20 °C

2.1: pyridine / 5 h / 0 - 20 °C

3.1: pyridine

4.1: acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: copper(II) bis(trifluoromethanesulfonate) / dichloromethane / 20 °C / Inert atmosphere

6.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -20 °C / Molecular sieves acid washed

7.1: sodium methylate; methanol / 0.33 h / 20 °C / Inert atmosphere

8.1: hydrogen / palladium on carbon / methanol / 1 h / 20 °C

With pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium methylate; acetic acid; palladium on carbon; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1207538-28-0
C₂₀H₃₅N₃O₉Si

: 1207538-22-4
α(1,2),α(1,6)-pseudomannotriose

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: copper(II) bis(trifluoromethanesulfonate) / dichloromethane / 20 °C / Inert atmosphere

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.33 h / -20 °C / Molecular sieves acid washed

4.1: sodium methylate; methanol / 0.33 h / 20 °C / Inert atmosphere

5.1: hydrogen / palladium on carbon / methanol / 1 h / 20 °C

With methanol; trimethylsilyl trifluoromethanesulfonate; hydrogen; sodium methylate; acetic acid; palladium on carbon; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; methanol; dichloromethane;