1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Base Information

Chemical Name:1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene
CAS No.:1160553-91-2
Molecular Formula:C₂₀H₂₇BO₂Si
Molecular Weight:338.33
Hs Code.:

Synonyms:1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

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Technology Process of 1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

There total 3 articles about 1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1296939-27-9
2-[2-(dimethylphenylsilyl)phenyl]-2,3-dihydrobenzo[d][1,3,2]diazaborinin-4(1H)-one

: 1160553-91-2
1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 17h; Inert atmosphere;
DOI:10.1021/ol200764g

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1160553-79-6
C₆H₄B(N₃HC₉H₆)Si(CH₃)2C₆H₅

: 1160553-91-2
1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; toluene; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 98-80-6
phenylboronic acid

: 1160553-91-2
1-dimethylphenylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 1 h / Inert atmosphere; Reflux

2: carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene / toluene / 3 h / 135 °C / Inert atmosphere

3: toluene-4-sulfonic acid / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); norbornene; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1021/ol200764g