5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE

Base Information

• Chemical Name: 5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE
• CAS No.: 30685-66-6
• Molecular Formula: C13H16 I N5 O3
• Molecular Weight: 417.206
• Mol file: 30685-66-6.mol

Synonyms:Adenosine,5'-deoxy-5'-iodo-2',3'-O-isopropylidene- (7CI,8CI); Furo[3,4-d]-1,3-dioxole,adenosine deriv.

Chemical Property of 5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE

Chemical Property:

• Boiling Point: 582.4±60.0 °C(Predicted)
• PKA: 3.56±0.10(Predicted)
• PSA: 97.31000
• Density: 2.19±0.1 g/cm3(Predicted)
• LogP: 1.84220

Purity/Quality:

97% ^*data from raw suppliers

5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE

There total 7 articles about 5'-DEOXY-2',3'-O-ISOPROPYLIDENE-5'-IODO-ADENOSINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2',3'-isopropylidene adenosine (362-75-4) → 2',3'-di-O-isopropylidene-5',N3-anhydro-5'-deoxyadenosine + 5'-iodo-5'-deoxy-2',3'-O-isopropylideneadenosine (30685-66-6)

Guidance literature:

With PS-Ph₃P; iodine; In pyridine; at 50 ℃;

DOI:10.1021/jm070362i

Reference yield: 75.0%

5'-iodo-5'-deoxy-2',3'-O-isopropylideneadenosine N1-oxide (72525-44-1) → 5'-iodo-5'-deoxy-2',3'-O-isopropylideneadenosine (30685-66-6)

Guidance literature:

With hydrogen; Ra-Ni; In methanol; for 6h;

DOI:10.1021/jo01293a005

Reference yield: 35.0%

2',3'-isopropylidene adenosine (362-75-4) → 5'-iodo-5'-deoxy-2',3'-O-isopropylideneadenosine (30685-66-6)

Guidance literature:

With methyltriphenoxyphosphonium iodide; In dichloromethane; for 2h; Ambient temperature;

upstream raw materials:

2',3'-isopropylidene adenosine

5'-iodo-5'-deoxy-2',3'-O-isopropylideneadenosine N¹-oxide

5'-O-(p-toluenesulfonyl)-2',3'-O'-isopropylideneadenosine N¹-oxide

2',3'-isopropylideneadenosine-1-oxide

Downstream raw materials:

5'-iodo-5'-deoxyadenosine

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