tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

Base Information

Chemical Name:tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)
CAS No.:16743-46-7
Molecular Formula:C₂₉H₂₂CrO₄P₂
Molecular Weight:548.435
Hs Code.:

Synonyms:tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

There total 10 articles about tetracarbonyl-bis(diphenylphosphino)methane-chromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 2071-20-7
bis-diphenylphosphinomethane

: 16743-46-7
tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

Guidance literature:: In diethylene glycol; mixt. Cr(CO)6 and bis(diphenylphosphino)methane in diglyme was heated at 135°C for 3.5 h;
DOI:10.1021/om990977g

Reference yield: 55.0%

: 64345-29-5
[Pd2Cl2(μ-bis(diphenylphosphino)methane)2]

: disodium decacarbonyldichromate

: 16743-46-7
tetracarbonyl-bis(diphenylphosphino)methane-chromium(0)

: 16924-36-0
N(CH₂CH₃)4⁽¹⁺⁾*[Cr₂(H)(CO)10]^(1-)=N(CH₂CH₃)4[Cr₂(H)(CO)10]

: Pd2(μ-CO)Cl2(μ-bis(diphenylphosphino)methane)

Guidance literature:: In tetrahydrofuran; (under N2) THF is added at -40°C to a solid mixt. of Pd complex and Na2Cr2(CO)10, mixt. is warmed to room temp. and then stirred for 2 h; evapn. to dryness, extn. with toluene, filtration through Celite on a glass frit, identification of soln. by IR and (31)P NMR;
DOI:10.1016/S0022-328X(00)99783-3

Reference yield: 54.0%

: 13007-92-6,199620-14-9
chromium hexacarbonyl

: 2071-20-7
bis-diphenylphosphinomethane

: 16743-46-7
(C₆H₅)2PCH₂P(C₆H₅)2Cr(CO)4

Guidance literature:: With sodium tetrahydroborate; In butan-1-ol; at 105 ℃; for 0.333333h; under 760.051 Torr; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1016/j.inoche.2012.09.030