(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

Base Information

Chemical Name:(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide
CAS No.:245092-69-7
Molecular Formula:C₁₆H₂₁NO₃S
Molecular Weight:307.414
Hs Code.:

Synonyms:(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

Chemical Property:

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Technology Process of (1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

There total 3 articles about (1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 245092-59-5
(1R,4R)-acetic acid 4-[but-3-enyl(toluene-4-sulfonyl)amino]cyclopent-2-enyl ester

: 245092-69-7
(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

Guidance literature:: With methanol; triethylamine; at 25 ℃; for 18h;
DOI:10.1016/S0040-4020(99)00299-9

Reference yield:

: 10285-80-0
N-tosyl-3-butenylamine

: 245092-69-7
(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / tributylphosphine; azodicarboxylic dipiperidine / benzene / 24 h

2: 96 percent / NEt₃; CH₃OH / 18 h / 25 °C

With methanol; tributylphosphine; triethylamine; 1,1'-azodicarbonyl-dipiperidine; In benzene; 1: Mitsunobu reaction / 2: Hydrolysis;
DOI:10.1016/S0040-4020(99)00299-9

Reference yield:

: 60410-16-4
(1R,4S)-4-hydroxy-2-cyclopentene-1-yl acetate

: 245092-69-7
(1R,4R)-N-but-3-enyl-N-(4-hydroxycyclopent-2-enyl)-4-methylbenzene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / tributylphosphine; azodicarboxylic dipiperidine / benzene / 24 h

2: 96 percent / NEt₃; CH₃OH / 18 h / 25 °C

With methanol; tributylphosphine; triethylamine; 1,1'-azodicarbonyl-dipiperidine; In benzene; 1: Mitsunobu reaction / 2: Hydrolysis;
DOI:10.1016/S0040-4020(99)00299-9