Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Base Information

Chemical Name:Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate
CAS No.:123910-97-4
Molecular Formula:C₃₁H₄₃N₅O₇
Molecular Weight:597.712
Hs Code.:

Synonyms:Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

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Chemical Property of Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

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Technology Process of Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

There total 4 articles about Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 123910-96-3
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

: 123910-97-4
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In trifluoroacetic acid; for 24h; under 2585.7 Torr;
DOI:10.1021/jo00297a044

Reference yield:

: 1118-89-4
diethyl-L-glutamate hydrochloride

: 123910-97-4
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / phenyl N-phenylphosphoramidochloridate, N-methylmorpholine, N-methylpyrrolidinone / 24 h / Ambient temperature

2: 100 percent / hydrogen / 5percent Pd/C / trifluoroacetic acid / 24 h / 2585.7 Torr

With 4-methyl-morpholine; 1-methyl-pyrrolidin-2-one; hydrogen; Phenyl N-phenylphosphoramidochloridate; palladium on activated charcoal; In trifluoroacetic acid;
DOI:10.1021/jo00297a044

Reference yield:

: 123910-94-1
4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoic acid

: 123910-97-4
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / phenyl N-phenylphosphoramidochloridate, N-methylmorpholine, N-methylpyrrolidinone / 24 h / Ambient temperature

2: 100 percent / hydrogen / 5percent Pd/C / trifluoroacetic acid / 24 h / 2585.7 Torr

With 4-methyl-morpholine; 1-methyl-pyrrolidin-2-one; hydrogen; Phenyl N-phenylphosphoramidochloridate; palladium on activated charcoal; In trifluoroacetic acid;
DOI:10.1021/jo00297a044