(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

Base Information

Chemical Name:(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide
CAS No.:672328-67-5
Molecular Formula:C₁₈H₂₃BrN₂O₂
Molecular Weight:379.297
Hs Code.:

Synonyms:(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

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Chemical Property of (2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

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Technology Process of (2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

There total 4 articles about (2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 672328-58-4
(2S)-N-(cyanomethyl)-2-hydroxy-4-methylpentanamide

: 1374991-94-2
1-(4-bromophenyl)-2-methylprop-2-enyl 2,2,2-trichloroethanimidoate

: 672328-67-5
(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 72h;

Reference yield:

: 23596-90-9
1-(4-bromophenyl)-2-methylprop-2-en-1-ol

: 672328-67-5
(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / diethyl ether / 0.25 h / 20 °C

1.2: 1 h / 20 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane / 72 h / 20 °C

With pyridinium p-toluenesulfonate; sodium hydride; In diethyl ether; dichloromethane;

Reference yield:

: 13748-90-8,498-36-2
(S)-2-hydroxyl-3,3-dimethylbutyric acid

: 672328-67-5
(2S)-2-{[1-(4-bromophenyl)-2-methylprop-2-enyl]oxy}-N-(cyanomethyl)-4-methylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 18 h / 20 °C

2: pyridinium p-toluenesulfonate / dichloromethane / 72 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; pyridinium p-toluenesulfonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;