1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

Base Information

• Chemical Name: 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside
• CAS No.: 344549-36-6
• Molecular Formula: C₂₃H₂₉NO₉
• Molecular Weight: 463.485

Synonyms:1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

Chemical Property of 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

There total 2 articles about 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside (344549-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / benzene / 5 h / 100 °C / UV-irradiation

2: 78 percent / tributyltin hydride; 2,2'-azobisisobutyronitrile / benzene / 1 h / 80 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene;

DOI:10.1021/ja003879r

Reference yield:

1-p-methylphenyltelluro-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (183367-67-1) → 1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside (344549-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / benzene / 5 h / 100 °C / UV-irradiation

2: 78 percent / tributyltin hydride; 2,2'-azobisisobutyronitrile / benzene / 1 h / 80 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene;

DOI:10.1021/ja003879r

Reference yield: 100.0%

1-[(2,6-dimethylphenylimino)methyl]-2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside (344549-36-6) → 1-[(2,6-dimethylphenylimino)methyl]-3,4,6-tri-O-acetyl-D-glucal

Guidance literature:

at -20 ℃; for 120h;

DOI:10.1021/ja003879r

upstream raw materials:

2,6-dimethylphenyl isonitrile

1-p-methylphenyltelluro-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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