(4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide

Base Information

• Chemical Name: (4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide
• CAS No.: 1229022-01-8
• Molecular Formula: C₂₆H₄₀ClNO₃
• Molecular Weight: 450.062

Synonyms:(4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide

Chemical Property of (4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide

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Technology Process of (4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide

There total 1 articles about (4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

(Z)-3-chloro-2-[2-hydroxy-3-methylpheny]-N-methyl-prop-2-en-amine (1228964-29-1) + lyngbic acid (70607-97-5) → (4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide (1229022-01-8)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2010.03.004

Reference yield: 67.0%

(4E,7S)-N-[(Z)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide (1229022-01-8) → (4E,7S)-N-[(E)-3-chloro-2-(2-hydroxy-3-methylphenyl)allyl]-7-methoxy-N-methyl-tetradec-4-enamide

Guidance literature:

With benzophenone; In dichloromethane; at 20 ℃; for 8h; Irradiation;

DOI:10.1016/j.tet.2010.03.004

upstream raw materials:

(Z)-3-chloro-2-[2-hydroxy-3-methylpheny]-N-methyl-prop-2-en-amine

lyngbic acid

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