N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

Base Information

Chemical Name:N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)
CAS No.:78715-87-4
Molecular Formula:C₅₉H₉₁NO₄Si
Molecular Weight:906.461
Hs Code.:

Synonyms:N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

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Technology Process of N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

There total 8 articles about N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78715-86-3
erythro-1-O-benzoylceramide

: 58479-61-1
tert-butylchlorodiphenylsilane

: 78715-87-4
N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; 0 to 25 deg C, 10 min, then 50 deg C, 4 h;
DOI:10.1021/jo00335a015

Reference yield:

: 765-13-9
pentadec-1-yne

: 78715-87-4
N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) DIBAL-H / 2.) ether, toluene, warming from 5 to 23 deg C, 1 h

2: 1.27 g / 2 N HCl / tetrahydrofuran / 16 h / 25 °C

3: pyridine / 16 h / 25 °C

4: 95 percent / imidazole / dimethylformamide / 0 to 25 deg C, 10 min, then 50 deg C, 4 h

With pyridine; 1H-imidazole; hydrogenchloride; diisobutylaluminium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00335a015

Reference yield:

: 17363-90-5
p-nitrophenyl oleate

: 78715-87-4
N-oleoyl-1-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-D-sphingosine (erythro form)

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h / 25 °C

2: 95 percent / imidazole / dimethylformamide / 0 to 25 deg C, 10 min, then 50 deg C, 4 h

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1021/jo00335a015