p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside
• CAS No.: 1040752-07-5
• Molecular Formula: C₃₅H₅₄Cl₃NO₆SSi₂
• Molecular Weight: 779.413

Synonyms:p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside

Chemical Property of p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside

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Technology Process of p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside

There total 1 articles about p-methylphenyl 6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylphenyl 2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-6-O-benzyl-1-thio-β-D-glucopyranoside (1040752-08-6) + t-butyldimethylsiyl triflate (69739-34-0) → p-methylphenyl 6-O-benzyl-3,4-di-O-tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside (1040752-07-5)

Guidance literature:

With dmap; In pyridine; at 60 ℃;

DOI:10.1039/b801305e

Reference yield: 85.0%

p-methylphenyl 6-O-benzyl-3,4-di-O-tbutyldimethylsilyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-1-thio-β-D-glucopyranoside (1040752-07-5) + phenyl 2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside (87470-73-3,120403-26-1,38184-12-2) → phenyl 6-O-(2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-6-O-benzyl-3,4-di-O-tbutyldimethylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside (1040752-10-0)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -45 ℃;

DOI:10.1039/b801305e

upstream raw materials:

p-methylphenyl 2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-6-O-benzyl-1-thio-β-D-glucopyranoside

t-butyldimethylsiyl triflate

Downstream raw materials:

phenyl 6-O-(2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-6-O-benzyl-3,4-di-O-^tbutyldimethylsilyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

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