[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

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Chemical Name:[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester
CAS No.:935553-22-3
Molecular Formula:C₃₄H₅₅N₂O₁₀P
Molecular Weight:682.792
Hs Code.:

Synonyms:[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

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Chemical Property of [11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

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Technology Process of [11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

There total 3 articles about [11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-53-8
1-dodecyl alcohol

: C₂₂H₃₀ClN₂O₉P

: 935553-22-3
[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1016/j.chemphyslip.2006.06.018

Reference yield:

: [11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid mono-(4-nitro-phenyl) ester

: 935553-22-3
[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 18 h / Heating

2: Et₃N / CH₂Cl₂ / 8 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.chemphyslip.2006.06.018

Reference yield:

: 268227-43-6
ethyl (4-nitrophenyl)[11-([(2,5-dioxotetrahydro-1H-1-pyrrolyl)oxy]carbonyloxy)undecyl]phosphonate

: 935553-22-3
[11-(2,5-dioxo-pyrrolidin-1-yloxycarbonyloxy)-undecyl]-phosphonic acid dodecyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (CH₃)3SiBr / CH₂Cl₂ / 40 h / 20 °C

2: oxalyl chloride; DMF / CH₂Cl₂ / 18 h / Heating

3: Et₃N / CH₂Cl₂ / 8 h / 20 °C

With oxalyl dichloride; trimethylsilyl bromide; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.chemphyslip.2006.06.018