N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester
CAS No.:1202249-78-2
Molecular Formula:C₂₈H₂₉FNO₄P
Molecular Weight:493.515
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

There total 1 articles about N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 2-(diphenylphosphanyl)-4-fluorophenol

: 1202249-78-2
N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200900692

Reference yield: 87.0%

: 1202249-78-2
N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester

: 66347-26-0
β-L-fucopyranosyl azide

: 2438-80-4,478518-52-4
L-Fucose

: 1202249-91-9
N-(N-tert-butoxycarbonyl-L-prolyl)-β-L-fucopyranosylamine

Guidance literature:: N-(tert-butoxycarbonyl)-L-proline 2-(diphenylphosphanyl)-4-fluorophenyl ester; β-L-fucopyranosyl azide; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692