[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

Base Information

• Chemical Name: [Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2
• CAS No.: 86943-72-8
• Molecular Formula: 2BF₄*C₆₂H₅₀Ir₂N₂O₂P₄
• Molecular Weight: 1537.04

Synonyms:[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

Chemical Property of [Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

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Technology Process of [Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

There total 2 articles about [Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)2(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Ir(C8H12)(((C6H5)2P)2CHC5H4N)](1+)*BF4(1-)=[Ir(C8H12)(((C6H5)2P)2CHC5H4N)]BF4 (86953-30-2) → [Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](2+)*2BF4(1-)=[Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](BF4)2 (86943-72-8) + [Ir2(CO)3(((C6H5)2P)2CHC5H4N)2](2+)*2BF4(1-)=[Ir2(CO)3(((C6H5)2P)2CHC5H4N)2](BF4)2 (86943-70-6)

Guidance literature:

With CO; In acetone; react. of acetone soln. of Ir complex with CO (1 atm) at room temp.; layered with pentane, crystals sepd.; elem. anal.;

Reference yield:

[Ir2(CO)3(((C6H5)2P)2CHC5H4N)2](2+)*2BF4(1-)=[Ir2(CO)3(((C6H5)2P)2CHC5H4N)2](BF4)2 (86943-70-6) → [Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](2+)*2BF4(1-)=[Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](BF4)2 (86943-72-8)

Guidance literature:

In acetone; byproducts: CO; purging acetone soln. of educt with N2; crystd. by layering with pentane; elem. anal.;

Reference yield: 78.0%

[Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](2+)*2BF4(1-)=[Ir2(CO)2(((C6H5)2P)2CHC5H4N)2](BF4)2 (86943-72-8) + tetra-(n-butyl)ammonium iodide (311-28-4) → [Ir2(CO)2I(((C6H5)2P)2CHC5H4N)2](1+)*BF4(1-)*CH2Cl2=[Ir2(CO)2I(((C6H5)2P)2CHC5H4N)2]BF4*CH2Cl2 (86943-76-2)

Guidance literature:

With CH₂Cl₂; In acetone; under N2, 1 equiv. of NBu4I dissolved in acetone added to acetone soln.of Ir complex; evapd. in vac., solid washed with H2O, crystals recrystd. from CH2Cl2/hexane; elem. anal.;

upstream raw materials:

[Ir(C₈H₁₂)(((C₆H₅)2P)2CHC₅H₄N)]⁽¹⁺⁾*BF₄^(1-)=[Ir(C₈H₁₂)(((C₆H₅)2P)2CHC₅H₄N)]BF₄

[Ir₂(CO)3(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)3(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

Downstream raw materials:

[Ir₂(CO)3(((C₆H₅)2P)2CHC₅H₄N)2]⁽²⁺⁾*2BF₄^(1-)=[Ir₂(CO)3(((C₆H₅)2P)2CHC₅H₄N)2](BF₄)2

[Ir₂(CO)2I(((C₆H₅)2P)2CHC₅H₄N)2]⁽¹⁺⁾*BF₄^(1-)*CH₂Cl₂=[Ir₂(CO)2I(((C₆H₅)2P)2CHC₅H₄N)2]BF₄*CH₂Cl₂

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