4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

Base Information

• Chemical Name: 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide
• CAS No.: 134248-33-2
• Molecular Formula: C₂₀H₁₇N₅O₂
• Molecular Weight: 359.387

Synonyms:4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

Chemical Property of 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

Chemical Property:

Purity/Quality:

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Technology Process of 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide

There total 3 articles about 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate (134248-29-6) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide (134248-33-2)

Guidance literature:

With hydrazine hydrate; In ethanol; for 8h; Heating;

Reference yield:

4-(1'H-indol-3'-ylmethylene)-2-methyl-5(4H)oxazolone (54753-57-0,70082-68-7,70082-69-8) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide (134248-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 0.33 h / 140 °C

2: 75 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

With hydrazine hydrate; In ethanol;

Reference yield:

4-methoxycarbonyl aniline (619-45-4) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoic acid hydrazide (134248-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 0.33 h / 140 °C

2: 75 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

With hydrazine hydrate; In ethanol;

upstream raw materials:

Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-2-methyl-5-oxo-1H-imidazol-1-yl>benzoate

4-(1'H-indol-3'-ylmethylene)-2-methyl-5(4H)oxazolone

4-methoxycarbonyl aniline

Downstream raw materials:

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(3,4-dimethoxy-phenyl)-1-o-tolylazo-meth-(E)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-2-methyl-5-oxo-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(3-chloro-phenylazo)-1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-hydrazide

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