1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane
CAS No.:226420-39-9
Molecular Formula:C₄₄H₅₆N₈O₄
Molecular Weight:760.98
Hs Code.:

Synonyms:1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Suppliers and Price of 1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

There total 3 articles about 1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2945-03-1
N-benzyl-2-bromoacetamide

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 226420-39-9
1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: With triethylamine; In tetrahydrofuran; for 7h; Heating;
DOI:10.1039/a809459d

Reference yield: 45.0%

: 64297-96-7
N-(iodoacetyl)benzylamine

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 226420-39-9
1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: 1,4,7,10-tetraazacyclododecan; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 45 ℃; for 0.166667h;

N-(iodoacetyl)benzylamine; In acetonitrile; at 45 ℃; for 24h;
DOI:10.1139/cjc-2012-0358

Reference yield:

: 100-46-9
benzylamine

: 226420-39-9
1,4,7,10-tetrakis[(N-benzylcarbamoyl)methyl]-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 24 h / 0 - 20 °C

2.1: sodium iodide / acetone / 24 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.17 h / 45 °C

3.2: 24 h / 45 °C

With sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile; 2.1: |Finkelstein Reaction;
DOI:10.1139/cjc-2012-0358