γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis

Base Information

• Chemical Name: γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis
• CAS No.: 78002-59-2
• Molecular Formula: C₈H₉ClO₂
• Molecular Weight: 172.611
• Mol file: 78002-59-2.mol

Synonyms:γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis

Chemical Property of γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis

There total 11 articles about γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

(dichloro-2,3-cyclohexenyl-6)acetate de methyle (69448-04-0,69448-05-1) → γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis (78002-59-2) + (dichloro-2,3cyclohexenyl-6)acete de methyle (69448-04-0,69448-05-1) + (dichloro-2,3cyclohexenyl-4)acete de methyle (69448-02-8,69448-03-9) + (dichloro-2,3cyclohexenyl-4)acete de methyle-trans (69448-02-8,69448-03-9)

Guidance literature:

at 160 ℃; for 5h;

Reference yield: 14.0%

(dichloro-2,3cyclohexenyl-4)acete de methyle (69448-02-8,69448-03-9) → γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis (78002-59-2) + (dichloro-2,3-cyclohexenyl-6)acetate de methyle (69448-04-0,69448-05-1) + (dichloro-2,3cyclohexenyl-6)acete de methyle (69448-04-0,69448-05-1) + (dichloro-2,3cyclohexenyl-4)acete de methyle-trans (69448-02-8,69448-03-9)

Guidance literature:

at 160 ℃; for 2.5h; under 760 Torr;

Reference yield: 9.0%

(dichloro-2,3cyclohexenyl-4)acete de methyle-trans (69448-02-8,69448-03-9) → γ-lactone de l'acide(chloro-2hydroxy-3cyclohexenyl-4)acetique-cis (78002-59-2) + (dichloro-2,3-cyclohexenyl-6)acetate de methyle (69448-04-0,69448-05-1) + (dichloro-2,3cyclohexenyl-6)acete de methyle (69448-04-0,69448-05-1) + (dichloro-2,3cyclohexenyl-4)acete de methyle (69448-02-8,69448-03-9)

Guidance literature:

at 160 ℃; for 6h; under 760 Torr;

upstream raw materials:

acides(dichloro-6,6-bicyclo<3.1.0>hexyl-2)acetiques

((1R,2R,5S)-6,6-Dichloro-bicyclo[3.1.0]hex-2-yl)-acetic acid

(dichloro-6,6 bicyclo<3.1.0>hexyl-2)acetates de methyle

((1R,2R,5S)-6,6-Dichloro-bicyclo[3.1.0]hex-2-yl)-acetic acid methyl ester

Downstream raw materials:

cis-hexahydrobenzofuran-2(3H)-one

(dichloro-2,3cyclohexenyl-4)acete de methyle

(dichloro-2,3cyclohexenyl-6)acete de methyle

(hydroxy-2 cyclohexyl)acetate de methyle-cis