C₂₅H₃₂O₅Si

Base Information

Chemical Name:C₂₅H₃₂O₅Si
CAS No.:1350623-75-4
Molecular Formula:C₂₅H₃₂O₅Si
Molecular Weight:440.612
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>5</sub>Si

Synonyms:C₂₅H₃₂O₅Si

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Chemical Property of C₂₅H₃₂O₅Si

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Technology Process of C₂₅H₃₂O₅Si

There total 16 articles about C₂₅H₃₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₀O₅Si

: 1350623-75-4
C₂₅H₃₂O₅Si

Guidance literature:: With quinoline; hydrogen; In ethyl acetate; at 20 ℃; for 0.5h;
DOI:10.1021/ol2028256

Reference yield:

: 1350623-74-3
C₂₈H₃₈O₅Si₂

: 1350623-75-4
C₂₅H₃₂O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran; water / 6.6 h / 0 - 20 °C

2: quinoline; hydrogen / ethyl acetate / 0.5 h / 20 °C

With quinoline; hydrogen; lithium hydroxide; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/ol2028256

Reference yield:

: C₃₁H₅₈O₅Si₂

: 1350623-75-4
C₂₅H₃₂O₅Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium acetate; pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Molecular sieve; Inert atmosphere

2.1: lithium trimethylsilylacetylenide / tetrahydrofuran; hexane / 0.88 h / -78 °C / Inert atmosphere

3.1: pyridine hydrogenfluoride / tetrahydrofuran / 4.8 h / -5 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 9.6 h / 20 °C / Inert atmosphere

5.1: zinc(II) chloride / tetrahydrofuran; diethyl ether / 0.25 h / -78 °C / Inert atmosphere

5.2: 0.75 h / -78 °C / Inert atmosphere

6.1: trifluoroacetic acid / diethyl ether / 10 h / 0 °C

7.1: pyridine hydrogenfluoride / tetrahydrofuran / 0 °C

8.1: tributylphosphine / acetonitrile / -40 °C / Inert atmosphere

9.1: triethylamine / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

9.2: 0.83 h / -5 °C / Inert atmosphere

10.1: 2,4,6-trimethyl-pyridine / dichloromethane / -20 °C / Inert atmosphere

11.1: lithium hydroxide / tetrahydrofuran; water / 6.6 h / 0 - 20 °C

12.1: quinoline; hydrogen / ethyl acetate / 0.5 h / 20 °C

With 2,4,6-trimethyl-pyridine; quinoline; tributylphosphine; hydrogen; lithium trimethylsilylacetylenide; sodium acetate; pyridine hydrogenfluoride; triethylamine; pyridinium chlorochromate; trifluoroacetic acid; zinc(II) chloride; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile;
DOI:10.1021/ol2028256