3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide

Base Information

• Chemical Name: 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide
• CAS No.: 1093115-86-6
• Molecular Formula: C₂₉H₂₈N₄O₇
• Molecular Weight: 544.564

Synonyms:3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide

Chemical Property of 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide

Chemical Property:

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Technology Process of 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide

There total 1 articles about 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C29H26N4O7 → 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide (1093115-86-6)

Guidance literature:

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; water; at 0 ℃; for 1h; pH=1 - 2; regioselective reaction; Molecular sieve;

DOI:10.1016/j.carres.2008.08.024

Reference yield:

3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide (70831-94-6) + 3-O-benzyl-2-deoxy-6-O-(p-methoxybenzyl)-2-phthalimido-β-D-glucopyranosyl azide (1093115-86-6) → C49H47N5O16

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; at -50 - 20 ℃; Molecular sieve;

DOI:10.1016/j.carres.2008.08.024

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