2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

Base Information

Chemical Name:2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester
CAS No.:1403821-14-6
Molecular Formula:C₄₂H₄₆O₈
Molecular Weight:678.822
Hs Code.:

Synonyms:2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

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Chemical Property of 2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

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Technology Process of 2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

There total 3 articles about 2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1157983-47-5
2-(4-(methoxy)benzyloxy)butyric acid

: 1403821-13-5
(S,S)-1,6-diphenyl-hexa-2,4(Z,Z)-diene-1,6-diol

: 1403821-14-6
2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol302567f

Reference yield:

: 4187-87-5,61317-73-5,64937-86-6,64599-56-0
1-phenylprop-2-yn-1-ol

: 1403821-14-6
2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: oxygen; N,N,N,N,-tetramethylethylenediamine / acetone / 14 h / 40 °C

2: zinc; copper(II) acetate monohydrate; silver nitrate / methanol; water / 36 h / 40 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere

With dmap; N,N,N,N,-tetramethylethylenediamine; oxygen; copper(II) acetate monohydrate; silver nitrate; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane; water; acetone;
DOI:10.1021/ol302567f

Reference yield:

: 197781-95-6
(R,R)-1,6-diphenyl-hexa-2,4-diyne-1,6-diol

: 1403821-14-6
2-(4-(methoxy)benzyloxy)butyric acid (S,S)-6-[2-(4-(methoxy)benzyloxy)-butyryloxy]-1,6-diphenylhexa-(Z,Z)-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; copper(II) acetate monohydrate; silver nitrate / methanol; water / 36 h / 40 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere

With dmap; copper(II) acetate monohydrate; silver nitrate; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane; water;
DOI:10.1021/ol302567f