C₅₀H₇₇IO₆Si₂

Base Information

Chemical Name:C₅₀H₇₇IO₆Si₂
CAS No.:1443051-52-2
Molecular Formula:C₅₀H₇₇IO₆Si₂
Molecular Weight:957.233
Hs Code.:

C<sub>50</sub>H<sub>77</sub>IO<sub>6</sub>Si<sub>2</sub>

Synonyms:C₅₀H₇₇IO₆Si₂

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Chemical Property of C₅₀H₇₇IO₆Si₂

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Technology Process of C₅₀H₇₇IO₆Si₂

There total 10 articles about C₅₀H₇₇IO₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1443051-53-3
C₄₃H₆₆O₆Si₂

: 216493-79-7
(E)-(3R,4R)-6-iodo-4-methyl-5-hexen-3-ol

: 1443051-52-2
C₅₀H₇₇IO₆Si₂

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2013.04.023

Reference yield:

: 1443051-56-6
C₃₄H₄₈O₄Si

: 1443051-52-2
C₅₀H₇₇IO₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: Dess-Martin periodane; sodium hydrogencarbonate / 0 °C

2: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C

3: 2,6-dimethylpyridine / dichloromethane

4: sodium tetrahydroborate / methanol / 3 h / 20 °C

5: Dess-Martin periodane / dichloromethane / 1 h

6: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol; water

7: 2,4,6-trichlorobenzoyl chloride; triethylamine; dmap / toluene / 2 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; (-)-sparteine; In methanol; dichloromethane; water; toluene; tert-butyl alcohol; 7: |Yamaguchi Lactonization;
DOI:10.1016/j.tetlet.2013.04.023

Reference yield:

: C₃₄H₄₆O₄Si

: 1443051-52-2
C₅₀H₇₇IO₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C

2: 2,6-dimethylpyridine / dichloromethane

3: sodium tetrahydroborate / methanol / 3 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 1 h

5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol; water

6: 2,4,6-trichlorobenzoyl chloride; triethylamine; dmap / toluene / 2 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; titanium tetrachloride; Dess-Martin periodane; triethylamine; (-)-sparteine; In methanol; dichloromethane; water; toluene; tert-butyl alcohol; 6: |Yamaguchi Lactonization;
DOI:10.1016/j.tetlet.2013.04.023