2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid

Base Information

• Chemical Name: 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid
• CAS No.: 80243-65-8
• Molecular Formula: C₁₇H₁₈N₂O₇
• Molecular Weight: 362.339

Synonyms:2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid

Chemical Property of 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid

Chemical Property:

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Technology Process of 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid

There total 2 articles about 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Amino-3-{4-[3-[4-(2-amino-2-carboxy-ethyl)-phenoxy]-5-((R)-amino-carboxy-methyl)-2-hydroxy-phenoxy]-phenyl}-propionic acid (70984-38-2,80299-49-6) → β-cyclohexylalanine (4441-50-3,27527-05-5,55658-63-4,58717-02-5) + 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid (80243-65-8)

Guidance literature:

With hydrogen;

DOI:10.1021/ja00365a098

Reference yield:

ristocetin A aglicone (73201-25-9,97371-83-0) → 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid (80243-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 57percent HI, P red / 22 h / 106 °C

2: H₂

With phosphorus; hydrogen iodide; hydrogen;

DOI:10.1021/ja00365a098

Reference yield:

sodium salicylate (3116-83-4) + 2-Amino-3-{4-[5-(amino-carboxy-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-propionic acid (80243-65-8) → 3-{4-[5-(Carboxy-{[1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-amino}-methyl)-2,3-dihydroxy-phenoxy]-phenyl}-2-{[1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-amino}-propionic acid

Guidance literature:

In methanol;

DOI:10.1021/ja00365a098

upstream raw materials:

2-Amino-3-{4-[3-[4-(2-amino-2-carboxy-ethyl)-phenoxy]-5-((R)-amino-carboxy-methyl)-2-hydroxy-phenoxy]-phenyl}-propionic acid

ristocetin A aglicone

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