(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

Base Information

Chemical Name:(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide
CAS No.:1434517-68-6
Molecular Formula:Br*C₄₂H₅₈N₂O₂P
Molecular Weight:733.812
Hs Code.:

Synonyms:(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

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Chemical Property of (3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

Chemical Property:

Purity/Quality:

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Technology Process of (3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

There total 8 articles about (3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1434517-64-2
10-(1H-imidazol-1-yl)octadecanoic acid

: 51860-45-8
3-hydroxypropyltriphenylphosphonium bromide

: 1434517-68-6
(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 95331-19-4
10-(benzyloxy)decane-1-ol

: 1434517-68-6
(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium chlorochromate / dichloromethane / 0 - 20 °C

2.1: magnesium; iodine / tetrahydrofuran / 70 °C

2.2: 0 - 20 °C

3.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

3.2: 16 h / 70 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 48 h / Reflux

5.1: Jones reagent / water; acetone / 0 - 20 °C

6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

With dmap; Jones reagent; palladium 10% on activated carbon; hydrogen; iodine; magnesium; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane; water; acetone;

Reference yield:

: 1434517-56-2
18-(benzyloxy)octadecan-9-ol

: 1434517-68-6
(3-((10-(1H-imidazol-1-yl)octadecanoyl)oxy)propyl)triphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

1.2: 16 h / 70 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol / 48 h / Reflux

3.1: Jones reagent / water; acetone / 0 - 20 °C

4.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

With dmap; Jones reagent; palladium 10% on activated carbon; hydrogen; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; acetone;