Technology Process of C37H36O6
There total 11 articles about C37H36O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
cyclohexylmagnesiumchloride;
With
zinc(II) chloride;
In
tetrahydrofuran; diethyl ether;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
3-benzyloxy-7-iodo-2-(4-benzyloxy-3,5-dimethoxy-phenyl)-chromen-4-one;
bis(tris(4-methyl)phenylphosphine)palladium dichloride;
In
tetrahydrofuran; diethyl ether;
for 3h;
Inert atmosphere;
Reflux;
With
hydrogenchloride; water;
In
tetrahydrofuran; diethyl ether;
- Guidance literature:
-
With
dichlorobis(tri-O-tolylphosphine)palladium;
In
tetrahydrofuran; diethyl ether;
for 3h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dmap; triethylamine / dichloromethane
2.1: aluminum (III) chloride / chlorobenzene
3.1: potassium hydroxide / ethanol
4.1: sodium hydroxide; dihydrogen peroxide / water; methanol
5.1: potassium carbonate; potassium iodide / acetone
6.1: zinc(II) chloride / diethyl ether; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
6.2: 3 h / Inert atmosphere; Reflux
With
dmap; dihydrogen peroxide; potassium carbonate; triethylamine; potassium iodide; potassium hydroxide; sodium hydroxide; zinc(II) chloride;
aluminum (III) chloride;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; chlorobenzene; acetone;
6.2: Negishi Coupling Reaction;
