C₃₇H₄₈N₆O₉

Base Information

Chemical Name:C₃₇H₄₈N₆O₉
CAS No.:1425940-90-4
Molecular Formula:C₃₇H₄₈N₆O₉
Molecular Weight:720.823
Hs Code.:

C<sub>37</sub>H<sub>48</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₃₇H₄₈N₆O₉

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Chemical Property of C₃₇H₄₈N₆O₉

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Technology Process of C₃₇H₄₈N₆O₉

There total 9 articles about C₃₇H₄₈N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425940-89-1
C₃₈H₅₀N₆O₉

: 1425940-90-4
C₃₇H₄₈N₆O₉

Guidance literature:: With lithium hydroxide monohydrate; In methanol; water; at 0 - 20 ℃; for 4h;
DOI:10.1021/ol4002762

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 1425940-90-4
C₃₇H₄₈N₆O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C

2.1: triethylamine / dichloromethane / 5 h / 20 °C / Cooling with ice

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 3102.97 Torr

4.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

4.2: 8 h / Inert atmosphere; Reflux

5.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

7.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

With oxalyl dichloride; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762

Reference yield:

: 221539-54-4
N-(2-aminobenzoyl)-α-methylalanine methyl ester

: 1425940-90-4
C₃₇H₄₈N₆O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

1.2: 8 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Molecular sieve

4.1: lithium hydroxide monohydrate / methanol; water / 4 h / 0 - 20 °C

With lithium hydroxide monohydrate; chloroformic acid ethyl ester; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol4002762