7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

Base Information

Chemical Name:7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate
CAS No.:1448297-29-7
Molecular Formula:C₂₆H₂₇FN₄O₅S
Molecular Weight:526.589
Hs Code.:

Synonyms:7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

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Chemical Property of 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

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Technology Process of 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

There total 11 articles about 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448297-33-3
methyl 3-chloro-7-(2,2-dimethylpropionylamino)-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

: 1448297-29-7
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium formate; palladium 10% on activated carbon / ethanol / 1 h / Reflux; Inert atmosphere

2: sulfuric acid / methanol / 16 h / Reflux

3: dichloromethane; pyridine / 96 h / 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tertiary-butyl phosphonium tetrafluoroborate / 1,4-dioxane; dimethyl sulfoxide / 2.25 h / 95 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; tri-tertiary-butyl phosphonium tetrafluoroborate; ammonium formate; In 1,4-dioxane; pyridine; methanol; ethanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 351003-45-7
2-bromo-4-fluorobenzene-1-sulfonyl chloride

: 1448297-29-7
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; pyridine / 96 h / 20 °C

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tertiary-butyl phosphonium tetrafluoroborate / 1,4-dioxane; dimethyl sulfoxide / 2.25 h / 95 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tertiary-butyl phosphonium tetrafluoroborate; In 1,4-dioxane; pyridine; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1448297-34-4
methyl 7-(2,2-dimethylpropionylamino)-3-hydroxy-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

: 1448297-29-7
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonyl-amino]-10H-9-oxa-1,2-diazaphenanthrene-8-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: trichlorophosphate / 0.75 h / 95 °C

2: ammonium formate; palladium 10% on activated carbon / ethanol / 1 h / Reflux; Inert atmosphere

3: sulfuric acid / methanol / 16 h / Reflux

4: dichloromethane; pyridine / 96 h / 20 °C

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tertiary-butyl phosphonium tetrafluoroborate / 1,4-dioxane; dimethyl sulfoxide / 2.25 h / 95 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; palladium 10% on activated carbon; tri-tertiary-butyl phosphonium tetrafluoroborate; ammonium formate; trichlorophosphate; In 1,4-dioxane; pyridine; methanol; ethanol; dichloromethane; dimethyl sulfoxide;