3-Ethyl-4-fluorobenzaldehyde

Base Information

Chemical Name:3-Ethyl-4-fluorobenzaldehyde
CAS No.:370867-69-9
Molecular Formula:C9H9 F O
Molecular Weight:152.168
Hs Code.:2913000090
DSSTox Substance ID:DTXSID80447555
Wikidata:Q82266425
Mol file:370867-69-9.mol

Synonyms:3-ethyl-4-fluorobenzaldehyde;370867-69-9;3-ethyl-4-fluoro-benzaldehyde;Benzaldehyde, 3-ethyl-4-fluoro-;SCHEMBL3035961;DTXSID80447555;CS-0191454;EN300-2989623;Z1255357885

Suppliers and Price of 3-Ethyl-4-fluorobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Ethyl-4-fluorobenzaldehyde 95+%
5g
$ 1978.00

Apolloscientific
3-Ethyl-4-fluorobenzaldehyde
1g
$ 235.00

Apolloscientific
3-Ethyl-4-fluorobenzaldehyde
500mg
$ 167.00

AOBChem
3-ethyl-4-fluorobenzaldehyde 95%
1g
$ 139.00

AOBChem
3-ethyl-4-fluorobenzaldehyde 95%
5g
$ 497.00

AOBChem
3-ethyl-4-fluorobenzaldehyde 95%
25g
$ 1662.00

Alichem
3-Ethyl-4-fluorobenzaldehyde
5g
$ 684.32

Alichem
3-Ethyl-4-fluorobenzaldehyde
1g
$ 203.04

Total 7 raw suppliers

Chemical Property of 3-Ethyl-4-fluorobenzaldehyde

Chemical Property:

PSA：17.07000
LogP:2.20060
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:152.063743068
Heavy Atom Count:11
Complexity:136

Purity/Quality:

97% ^*data from raw suppliers

3-Ethyl-4-fluorobenzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=C(C=CC(=C1)C=O)F

Technology Process of 3-Ethyl-4-fluorobenzaldehyde

There total 5 articles about 3-Ethyl-4-fluorobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3-ethyl-4-fluorobenzyl alcohol

: 370867-69-9
3-ethyl-4-fluoro-benzaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.75h;
DOI:10.1021/jm010100v

Reference yield: 80.0%

: 627463-25-6
4-bromo-2-ethyl-1-fluoro-benzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 370867-69-9
3-ethyl-4-fluoro-benzaldehyde

Guidance literature:: 4-bromo-2-ethyl-1-fluoro-benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; at -78 ℃; for 1h;

Reference yield:

: 82702-31-6
methyl 3-bromo-4-fluorobenzoate

: 370867-69-9
3-ethyl-4-fluoro-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: ZnCl / diethyl ether; tetrahydrofuran / 3 h / 50 °C

1.2: PdCl₂(dppf); CuI / diethyl ether; tetrahydrofuran / 48 h / 20 °C

2.1: 3.5 g / LiAlH₄ / tetrahydrofuran / 1 h / 0 - 20 °C

3.1: 95 percent / (COCl)2; DMSO / CH₂Cl₂ / 0.75 h / -78 °C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; 3.1: Swern oxidation;
DOI:10.1021/jm010100v