7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one

Base Information

• Chemical Name: 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one
• CAS No.: 1439915-84-0
• Molecular Formula: C₄₃H₅₂N₂O₇
• Molecular Weight: 708.895

Synonyms:7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one

Chemical Property of 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one

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Technology Process of 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one

There total 3 articles about 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.4%

7-(4-bromobutoxy)-3-(4-(4-bromobutoxy)phenyl)-5-hydroxy-4H-chromen-4-one (1439920-42-9) + N-ethyl-N-[(2methoxyphenyl)methyl]amine (62924-83-8) → 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one (1439915-84-0)

Guidance literature:

With potassium carbonate; potassium iodide; In acetonitrile; at 60 - 65 ℃; Inert atmosphere;

DOI:10.1016/j.ejmech.2014.02.045

Reference yield:

5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on (446-72-0) → 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one (1439915-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium iodide; potassium carbonate / acetone / Reflux; Inert atmosphere

2: potassium iodide; potassium carbonate / acetonitrile / 60 - 65 °C / Inert atmosphere

With potassium carbonate; potassium iodide; In acetone; acetonitrile;

DOI:10.1016/j.ejmech.2014.02.045

Reference yield:

ortho-anisaldehyde (135-02-4) → 7-(4-(ethyl(2-methoxybenzyl)amino)butoxy)-3-(4-(4-(ethyl(2-methoxybenzyl)amino) butoxy)phenyl)-5-hydroxy-4H-chromen-4-one (1439915-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: potassium iodide; potassium carbonate / acetonitrile / 60 - 65 °C / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; potassium iodide; In methanol; acetonitrile;

DOI:10.1016/j.ejmech.2014.02.045

upstream raw materials:

7-(4-bromobutoxy)-3-(4-(4-bromobutoxy)phenyl)-5-hydroxy-4H-chromen-4-one

N-ethyl-N-[(2methoxyphenyl)methyl]amine

5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on

ortho-anisaldehyde

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