2-Methylisonicotinsaeure-p-toluidid

Base Information

• Chemical Name: 2-Methylisonicotinsaeure-p-toluidid
• CAS No.: 4593-14-0
• Molecular Formula: C₁₄H₁₄N₂O
• Molecular Weight: 226.278
• Mol file: 4593-14-0.mol

Synonyms:2-Methylisonicotinsaeure-p-toluidid

Chemical Property of 2-Methylisonicotinsaeure-p-toluidid

Chemical Property:

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Technology Process of 2-Methylisonicotinsaeure-p-toluidid

There total 1 articles about 2-Methylisonicotinsaeure-p-toluidid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-Methylisonicotinsaeure-p-toluidid (4593-14-0)

Guidance literature:

2-Methylisonicotinsaeure, p-Toluidin b. 130-140grad in Ggw. von POCl3 (S.43,44);

Reference yield: 88.0%

2-Methylisonicotinsaeure-p-toluidid (4593-14-0) + diphenyl acetylene (501-65-5) → C42H32N2O (1329663-73-1)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; In acetone; at 120 ℃; for 6h; Inert atmosphere; Sealed vessel;

DOI:10.1021/jo201266u

Reference yield: 58.0%

tert-Butyl acrylate (1663-39-4,25232-27-3) + 2-Methylisonicotinsaeure-p-toluidid (4593-14-0) → C21H22N2O3 (1389293-18-8)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; In acetonitrile; at 110 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c2ob25773d

Downstream raw materials:

C₄₂H₃₂N₂O

C₄₁H₂₉BrN₂O

C₂₁H₂₂N₂O₃