trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV)

Base Information

• Chemical Name: trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV)
• CAS No.: 26334-88-3
• Molecular Formula: C₄₄H₂₆Cl₄N₄O₂Sn
• Molecular Weight: 903.238

Synonyms:trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV)

Chemical Property of trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV)

Chemical Property:

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Technology Process of trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV)

There total 2 articles about trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10,15,20-tetrakis(4-chlorophenyl)porphyrin + tin(II) chloride dihdyrate (10025-69-1) → trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV) (26334-88-3)

Guidance literature:

5,10,15,20-tetrakis(4-chlorophenyl)porphyrin; tin(II) chloride dihdyrate; In ethanol; chloroform; for 4h; Reflux;

In ethanol; chloroform; triethylamine; for 0.0833333h;

DOI:10.1007/s10973-017-6531-x

Reference yield:

4-chlorobenzaldehyde (104-88-1) → trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV) (26334-88-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 0.67 h / Reflux

2.1: chloroform; ethanol / 4 h / Reflux

2.2: 0.08 h

In ethanol; chloroform;

DOI:10.1007/s10973-017-6531-x

Reference yield:

trans-dihydroxo(meso-5,10,15,20-tetra(p-chlorophenyl)porphyrinato)tin(IV) (26334-88-3) + C7H4O6S(2-)*H(1+) → C58H34Cl4N4O12S2Sn

Guidance literature:

In dichloromethane; at 20 ℃; for 24h;

DOI:10.1007/s10973-017-6531-x

upstream raw materials:

tin(II) chloride dihdyrate

4-chlorobenzaldehyde

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