(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

Base Information

Chemical Name:(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine
CAS No.:122992-86-3
Molecular Formula:C₂₅H₂₄ClNO₄
Molecular Weight:437.923
Hs Code.:

Synonyms:(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

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Chemical Property of (chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

Chemical Property:

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Technology Process of (chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

There total 4 articles about (chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 122992-85-2
(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 dihydro-3,4 isoquinoleine

: 122992-86-3
(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

Guidance literature:: With sodium tetrahydroborate; In methanol; chloroform; 1.) room temp. 30 min; 2.) reflux 30 min;

Reference yield:

: 40162-94-5
L'acide chloro-2 homopiperonylique

: 122992-86-3
(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / benzene / 2 h / Heating

2: 68 percent / diethyl ether / 0.25 h / 50 °C

3: 99 percent / POCl₃ / benzene / 1.5 h / Heating

4: 91 percent / NaBH₄ / methanol; CHCl₃ / 1.) room temp. 30 min; 2.) reflux 30 min

With sodium tetrahydroborate; thionyl chloride; trichlorophosphate; In methanol; diethyl ether; chloroform; benzene;

Reference yield:

: (6-Chloro-benzo[1,3]dioxol-5-yl)-acetyl chloride

: 122992-86-3
(chloro-2' methylenedioxy-4',5' benzyl)-1 benzyloxy-6 methoxy-7 tetrahydro-1,2,3,4 isoquinoleine

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / diethyl ether / 0.25 h / 50 °C

2: 99 percent / POCl₃ / benzene / 1.5 h / Heating

3: 91 percent / NaBH₄ / methanol; CHCl₃ / 1.) room temp. 30 min; 2.) reflux 30 min

With sodium tetrahydroborate; trichlorophosphate; In methanol; diethyl ether; chloroform; benzene;