9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

Base Information

Chemical Name:9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine
CAS No.:151055-69-5
Molecular Formula:C₄₇H₄₀N₄O₂
Molecular Weight:692.86
Hs Code.:

9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N<sup>6</sup>-triphenylmethyl-3-deazaadenine

Synonyms:9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

Chemical Property:

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Technology Process of 9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

There total 1 articles about 9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 76-83-5
trityl chloride

: 127853-26-3
9-(S)-(2,3-dihydroxypropyl)-3-deazaadenine

: 151055-69-5
9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 5h;
DOI:10.1135/cccc19931403

Reference yield:

: 151055-69-5
9-(S)-(2-hydroxy-3-triphenylmethoxypropyl)-N⁶-triphenylmethyl-3-deazaadenine

: 137427-72-6
cyclic ester of 9-(S)-(3-hydroxy-2-phosphonomethoxypropyl)-3-deazaadenine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride, 2.) aq. acetic acid / 1.) DMF, RT, 24 h, 2.) reflux, 30 min

2: 41 percent / bromotrimethylsilane / acetonitrile / 20 h / 20 °C

3: 94 percent / N,N'-dicyclohexylcarbodiimide, morpholino-N,N'-dicyclohexylguanidine / 2-methyl-propan-2-ol / 5 h / Heating

With trimethylsilyl bromide; morpholino-N,N'-dicyclohexylguanidine; sodium hydride; acetic acid; dicyclohexyl-carbodiimide; In acetonitrile; tert-butyl alcohol;
DOI:10.1135/cccc19931403