N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

Base Information

Chemical Name:N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester
CAS No.:637041-40-8
Molecular Formula:C₃₀H₄₁NO₄S
Molecular Weight:511.726
Hs Code.:

Synonyms:N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

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Technology Process of N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

There total 2 articles about N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 870-63-3
prenyl bromide

: 153764-25-1
N-tosylimine of (R)-8-phenylmenthylglyoxylate

: 637041-40-8
N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

Guidance literature:: prenyl bromide; With zinc; In tetrahydrofuran; at 0 ℃;

N-tosylimine of (R)-8-phenylmenthylglyoxylate; In tetrahydrofuran; at 0 ℃; for 12h;
DOI:10.1055/s-2003-41453

Reference yield:

: 4083-64-1
Tosyl isocyanate

: 637041-40-8
N-[(2'S)-N'-p-toluenesulfonyl-3',3'-dimethylallylglycine] 8-(R)-phenylmenthyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 24 h / Heating

2.1: Zn / tetrahydrofuran / 0 °C

2.2: 50 percent / tetrahydrofuran / 12 h / 0 °C

With zinc; In tetrahydrofuran; toluene; 2.2: Barbier addition;
DOI:10.1055/s-2003-41453