benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

Base Information

Chemical Name:benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside
CAS No.:136136-34-0
Molecular Formula:C₄₀H₄₆O₁₄
Molecular Weight:750.797
Hs Code.:

Synonyms:benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

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Technology Process of benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

There total 4 articles about benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 136136-33-9
benzyl 2,4-di-O-benzyl-β-D-xylopyranoside

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 136136-34-0
benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

Guidance literature:: With mercury(II) cyanide; In acetonitrile; at 40 ℃; for 2h;

Reference yield:

: 76490-96-5
benzyl 2,3-anhydro-4-O-benzyl-β-D-ribopyranoside

: 136136-34-0
benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / 7 h / 70 - 75 °C

2: 1.) NaH / 1.) 1,2-dimethoxyethane, 2.) 2 h

3: 70 percent / 10percent PdCl₂, sodium acetate / acetic acid; H₂O / 48 h / 70 °C

4: 84 percent / Hg(CN)2 / acetonitrile / 2 h / 40 °C

With sodium acetate; mercury(II) cyanide; sodium hydride; palladium dichloride; In water; acetic acid; acetonitrile;

Reference yield:

: 136136-31-7
benzyl 3-O-allyl-4-O-benzyl-β-D-xylopyranoside

: 136136-34-0
benzyl 2,4-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) 1,2-dimethoxyethane, 2.) 2 h

2: 70 percent / 10percent PdCl₂, sodium acetate / acetic acid; H₂O / 48 h / 70 °C

3: 84 percent / Hg(CN)2 / acetonitrile / 2 h / 40 °C

With sodium acetate; mercury(II) cyanide; sodium hydride; palladium dichloride; In water; acetic acid; acetonitrile;