C₅₃H₇₁NO₁₀SSi₂

Base Information

Chemical Name:C₅₃H₇₁NO₁₀SSi₂
CAS No.:922178-31-2
Molecular Formula:C₅₃H₇₁NO₁₀SSi₂
Molecular Weight:970.384
Hs Code.:

C<sub>53</sub>H<sub>71</sub>NO<sub>10</sub>SSi<sub>2</sub>

Synonyms:C₅₃H₇₁NO₁₀SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₁NO₁₀SSi₂

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Technology Process of C₅₃H₇₁NO₁₀SSi₂

There total 12 articles about C₅₃H₇₁NO₁₀SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 922178-23-2
(3aS,4S,5S,6R,7R,7aS)-6-(1-ethynyl)-2,2-dimethyl-7-[4-methylphenyl(propynyl)sulfonamido]-4,5-di(phenylcarbonyloxy)perhydro-1,3-benzodioxole

: 2,5-di(tert-butyldimethylsilyloxy)-3-hexyne

: 922178-31-2
C₅₃H₇₁NO₁₀SSi₂

Guidance literature:: dicarbonylcyclopentadienylcobalt; In xylene; at 140 ℃; for 42h;
DOI:10.1139/V06-078

Reference yield:

: 130669-75-9
(3aS,7aS)-4-bromo-2,2-dimethyl-3a,7a-dihydro-1,3-benzodioxole

: 922178-31-2
C₅₃H₇₁NO₁₀SSi₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: Cu(acac)2 / acetonitrile / 0 - 20 °C

2.1: n-Bu₃SnH; 2,2'-azobisisobutyronitrile / tetrahydrofuran / Heating

3.1: n-BuLi / toluene / 0.17 h / 0 °C

3.2: AlCl₃ / toluene / 18 h / 0 - 20 °C

4.1: 46 percent / N-methylmorpholine-N-oxide; OsO₄ / CH₂Cl₂ / 3 h / 20 °C

5.1: 80 percent / pyridine / 1.5 h / 20 °C

6.1: 76 percent / tetrabutylammoinum triphenyldifluorosilicate / acetonitrile / 1.5 h / 20 °C

7.1: 94 percent / sodium hexamethyldisilazide; tetrabutylammonium iodide / tetrahydrofuran / 0 - 20 °C

8.1: 31 percent / CpCo(CO)2 / xylene / 42 h / 140 °C

With pyridine; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; 4-methylmorpholine N-oxide; tetrabutylammonium triphenyldifluorosilicate; copper acetylacetonate; dicarbonylcyclopentadienylcobalt; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; xylene;
DOI:10.1139/V06-078

Reference yield:

: 67451-62-1,82683-92-9,132958-32-8,130792-45-9
cis-(1S,2S)-1,2-dihydroxy-3-bromocyclohexa-3,5-diene

: 922178-31-2
C₅₃H₇₁NO₁₀SSi₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: p-toluenesulfonic acid / acetone / 20 °C

2.1: Cu(acac)2 / acetonitrile / 0 - 20 °C

3.1: n-Bu₃SnH; 2,2'-azobisisobutyronitrile / tetrahydrofuran / Heating

4.1: n-BuLi / toluene / 0.17 h / 0 °C

4.2: AlCl₃ / toluene / 18 h / 0 - 20 °C

5.1: 46 percent / N-methylmorpholine-N-oxide; OsO₄ / CH₂Cl₂ / 3 h / 20 °C

6.1: 80 percent / pyridine / 1.5 h / 20 °C

7.1: 76 percent / tetrabutylammoinum triphenyldifluorosilicate / acetonitrile / 1.5 h / 20 °C

8.1: 94 percent / sodium hexamethyldisilazide; tetrabutylammonium iodide / tetrahydrofuran / 0 - 20 °C

9.1: 31 percent / CpCo(CO)2 / xylene / 42 h / 140 °C

With pyridine; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; tetrabutylammonium triphenyldifluorosilicate; copper acetylacetonate; dicarbonylcyclopentadienylcobalt; In tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile; xylene;
DOI:10.1139/V06-078