3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

Base Information

Chemical Name:3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose
CAS No.:175979-01-8
Molecular Formula:C₁₇H₂₄NO₆P
Molecular Weight:369.354
Hs Code.:

3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C-<methoxy(phenyl)phosphinyl>-α-D-xylofuranose

Synonyms:3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

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Chemical Property of 3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

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Technology Process of 3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

There total 4 articles about 3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 175979-00-7
Imidazole-1-carbothioic acid O-[((3aR,5S,6R,6aR)-6-acetylamino-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-(methoxy-phenyl-phosphinoyl)-methyl] ester

: 175979-01-8
3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; at 120 ℃; for 2h; Yield given;
DOI:10.1016/0008-6215(95)00356-8

Reference yield:

: 58700-31-5
3-acetamido-3-desoxy-1,2-O-isopropylidene-α-D-xylo-pentodialdo-1,4-furanose

: 175979-01-8
3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / Ambient temperature

2: 1,2-dichloro-ethane / 1 h / Ambient temperature

3: Bu₃SnH / toluene / 2 h / 120 °C

With tri-n-butyl-tin hydride; triethylamine; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/0008-6215(95)00356-8

Reference yield:

: 7162-15-4,111469-75-1,121467-78-5
methyl phenylphosphinate

: 175979-01-8
3-acetamido-3,5-dideoxy-1,2-O-isopropylidene-5-C--α-D-xylofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / Ambient temperature

2: 1,2-dichloro-ethane / 1 h / Ambient temperature

3: Bu₃SnH / toluene / 2 h / 120 °C

With tri-n-butyl-tin hydride; triethylamine; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/0008-6215(95)00356-8