((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine

Base Information

• Chemical Name: ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine
• CAS No.: 189350-53-6
• Molecular Formula: C₁₃H₁₂F₇N
• Molecular Weight: 315.234

Synonyms:((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine

Chemical Property of ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

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Technology Process of ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine

There total 2 articles about ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

[2,2,3,3,4,4,4-Heptafluoro-1-methyl-but-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine (189350-48-9) → ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine (189350-53-6)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 60 ℃; for 15h;

DOI:10.1021/jo970425c

Reference yield:

heptafluoropropyl methyl ketone (355-17-9) → ((R)-2,2,3,3,4,4,4-Heptafluoro-1-methyl-butyl)-[1-phenyl-eth-(E)-ylidene]-amine (189350-53-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 74 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / 15 h / 60 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene;

DOI:10.1021/jo970425c

upstream raw materials:

[2,2,3,3,4,4,4-Heptafluoro-1-methyl-but-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

heptafluoropropyl methyl ketone

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