(2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Name:(2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:1259018-25-1
Molecular Formula:C₂₇H₂₇ClN₂O₁₀S
Molecular Weight:607.038
Hs Code.:

Synonyms:(2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 1 articles about (2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1225430-43-2
2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(furan-2-yl)-1,3,4-thiadiazole

: 108-24-7
acetic anhydride

: 1259018-25-1
(2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(furan-2-yl)-1,3,4-thiadiazole; With trimethylsilyl iodide; In acetonitrile; at 50 ℃; Inert atmosphere;

With methanol; In acetonitrile; at 0 ℃; Inert atmosphere;

acetic anhydride; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

Reference yield: 58.0%

: 1259018-25-1
(2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1225430-76-1
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: (2S,3R,4R,5S,6S)-2-acetoxymethyl-6-(4-chloro-3-((5-(furan-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate; With sodium methylate; In methanol; at 20 ℃; for 2h; Inert atmosphere;

In methanol;