N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

Base Information

Chemical Name:N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine
CAS No.:1021388-28-2
Molecular Formula:C₁₈H₁₈F₂N₄O
Molecular Weight:344.364
Hs Code.:

Synonyms:N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

Chemical Property:

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Technology Process of N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

There total 3 articles about N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 3447-53-8
4-(difluoromethoxy)benzyl bromide

: 59591-76-3
N'-(1⁽²⁾H-indazol-3-yl)-N,N-dimethyl-formamidine

: 1021388-28-2
N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 50 ℃; for 16h;

Reference yield:

: 874-05-5
3-aminoindazole

: 1021388-28-2
N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 16 h / 20 °C

2: potassium tert-butylate / tetrahydrofuran / 16 h / 50 °C

With potassium tert-butylate; In tetrahydrofuran;

Reference yield:

: 394-47-8
2-fluorobenzonitrile

: 1021388-28-2
N'-[1-(4-difluoromethoxybenzyl)-1H-indazol-3-yl]-N,N-dimethylformamidine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / ethanol / 16 h / 20 °C / Heating / reflux

2: 16 h / 20 °C

3: potassium tert-butylate / tetrahydrofuran / 16 h / 50 °C

With potassium tert-butylate; hydrazine; In tetrahydrofuran; ethanol;