3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

Base Information

Chemical Name:3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride
CAS No.:1373433-85-2
Molecular Formula:C₁₈H₃₁N₂O₃*Cl
Molecular Weight:358.909
Hs Code.:

Synonyms:3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

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Chemical Property of 3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

Chemical Property:

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Technology Process of 3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

There total 6 articles about 3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1226913-37-6
benzyl 4-(dimethylamino)-2-methylbutan-2-ylcarbamate

: 6482-24-2
2-Bromoethyl methyl ether

: 1373433-85-2
3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

Guidance literature:: benzyl 4-(dimethylamino)-2-methylbutan-2-ylcarbamate; 2-Bromoethyl methyl ether; at 50 ℃; for 5h;

With silver(l) oxide; In water; for 0.5h;

With hydrogenchloride; In water;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 1373433-85-2
3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / water / 49 h / 20 - 95 °C

2.1: thionyl chloride / 1,2-dichloro-ethane / 2 h / 50 °C

3.1: dichloromethane; water / 1 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 20 - 70 °C / Cooling with ice

4.2: 0.33 h / Cooling with ice

4.3: 0.33 h

5.1: tetrahydrofuran / 17 h / 20 °C

6.1: 5 h / 50 °C

6.2: 0.5 h

With lithium aluminium tetrahydride; thionyl chloride; sodium azide; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;

Reference yield:

: 105090-72-0
3-azido-3-methylbutanoic acid

: 1373433-85-2
3-(((benzyloxy)carbonyl)amino)-N-(2-methoxyethyl)-N,N,3-trimethylbutan-1-aminium chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 1,2-dichloro-ethane / 2 h / 50 °C

2.1: dichloromethane; water / 1 h / 0 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 20 - 70 °C / Cooling with ice

3.2: 0.33 h / Cooling with ice

3.3: 0.33 h

4.1: tetrahydrofuran / 17 h / 20 °C

5.1: 5 h / 50 °C

5.2: 0.5 h

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;