ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside
CAS No.:173167-84-5
Molecular Formula:C₁₉H₂₈O₅S
Molecular Weight:368.494
Hs Code.:

Synonyms:ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

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Technology Process of ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

There total 2 articles about ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 127753-95-1
ethyl 2,3-O-isopropylidene-1-thio-α-L-rhamnopyranoside

: 824-94-2
p-methoxybenzyl chloride

: 173167-84-5
ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 48h;
DOI:10.1016/0008-6215(95)00182-S

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 127753-95-1
ethyl 2,3-O-isopropylidene-1-thio-α-L-rhamnopyranoside

: 173167-84-5
ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

Guidance literature:: With tetrabutylammomium bromide; sodium hydride; In N,N-dimethyl-formamide; 1.) r.t., 45 min, 2.) r.t., 2.5 h;
DOI:10.1002/jlac.199619961016

Reference yield: 75.0%

: p-methoxyphenyl (3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-(3-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→3)-4,6-di-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 173167-84-5
ethyl 2,3-O-isopropylidene-4-O-p-methoxybenzyl-1-thio-α-L-rhamnopyranoside

: p-methoxyphenyl (2,3-O-isopropylidene-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-(3-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→3)-4,6-di-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

Guidance literature:: With N-iodo-succinimide; perchloric acid adsorbed on silica gel; In dichloromethane; at -30 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2019.130697