N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide

Base Information

• Chemical Name: N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide
• CAS No.: 1616700-71-0
• Molecular Formula: C₃₉H₄₃N₇O₁₉
• Molecular Weight: 913.806

Synonyms:N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide

Chemical Property of N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide

Chemical Property:

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Technology Process of N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide

There total 1 articles about N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N3-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide (1407510-85-3) → N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N3-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide (1616700-71-0)

Guidance literature:

N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide; With pentamethylbenzene,; boron trichloride; In dichloromethane; at -78 ℃; for 1.5h; Inert atmosphere;

With methanol; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja503911p

Reference yield: 76.0%

(2S,5R,6R)-6-((R)-2-(hex-5-ynamido)-2-phenylacetamido)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid (1067890-47-4) + N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N3-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide (1616700-71-0) → C61H68N10O24S (1616700-77-6)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In 1,4-dioxane; water; dimethyl sulfoxide; at 20 ℃; for 2h;

DOI:10.1021/ja503911p

Reference yield: 66.0%

N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N3-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide (1616700-71-0) + (2S,5R,6R)-6-((R)-2-(hex-5-ynamido)-2-(4-hydroxyphenyl)acetamido)-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid (1616700-74-3) → C61H68N10O25S (1616700-78-7)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In 1,4-dioxane; water; dimethyl sulfoxide; at 20 ℃;

DOI:10.1021/ja503911p

upstream raw materials:

N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide

Downstream raw materials:

C₆₁H₆₈N₁₀O₂₄S

C₆₁H₆₈N₁₀O₂₅S

C₆₀H₇₀N₁₀O₂₃S

C₆₀H₇₀N₁₀O₂₄S

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