V⁽⁴⁺⁾Cl^(1-)N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

Base Information

Chemical Name:V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)
CAS No.:177778-19-7
Molecular Formula:C₂₄H₁₂F₁₅N₄*Cl*V
Molecular Weight:727.757
Hs Code.:

V<sup>(4+)</sup>*Cl<sup>(1-)</sup>*N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)3<sup>(3-)</sup>=VCl(N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)3)

Synonyms:V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

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Chemical Property of V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

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Technology Process of V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

There total 1 articles about V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 177778-11-9
HN(C₂H₅)3⁽¹⁺⁾*V⁽³⁺⁾*N(CH₂CH₂NC₆F₅)3^(3-)*Cl^(1-)=[HN(C₂H₅)3][(N(CH₂CH₂NC₆F₅)3)VCl]

: 177778-19-7
V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

Guidance literature:: With ((C₅H₅)2Fe)(CF₃SO₃); In dichloromethane; N2-atmosphere; slight excess oxidant, warming from -30°C to room temp., stirring for 20 h; filtration (Celite), evapn. (vac.), dissoln. in PhMe, crystn. (-30°C, overnight), recrystn. (CH2Cl2, -30°C), washing (cold PhMe), drying (vac.); elem. anal.;
DOI:10.1021/ic951433j

Reference yield: 80.0%

: 177778-19-7
V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

: 184649-32-9
V(N(CH₂CH₂NC₆F₅)3)

Guidance literature:: With sodium amalgam; In toluene; stirring at room temp. for 15 h; filtration (Celite), solvent removal (vac.), washing (pentane), drying (vac.); elem. anal.;
DOI:10.1021/ic960889d

Reference yield: 78.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 177778-19-7
V⁽⁴⁺⁾*Cl^(1-)*N(CH₂CH₂NC₆F₅)3^(3-)=VCl(N(CH₂CH₂NC₆F₅)3)

: 177778-15-3
V(N(CH₂CH₂NC₆F₅)3)(C₄H₈O)

Guidance literature:: With sodium amalgam; In tetrahydrofuran; N2-atmosphere; stirring for 12 h at room temp.; filtration (Celite), evapn. (vac.), extn. into cold ether, THF addn., concn., layering with pentane, crystn. (-30°C; two crops);
DOI:10.1021/ic951433j