(2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

Base Information

Chemical Name:(2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine
CAS No.:109361-22-0
Molecular Formula:C₁₃H₁₈NO₂P
Molecular Weight:251.265
Hs Code.:

Synonyms:(2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

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Technology Process of (2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

There total 2 articles about (2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 106-95-6
allyl bromide

: 89878-06-8
2-ethoxy-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidine

: 109242-43-5
(2R,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

: 109361-22-0
(2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

Guidance literature:: for 120h; Heating;

Reference yield:

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 109361-22-0
(2S,4S,5R)-3,4-Dimethyl-5-phenyl-2-(prop-2-enyl)-2-oxo-1,3,2-oxazaphospholidine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: 15 percent / 120 h / Heating

With triethylamine; In dichloromethane;