Technology Process of C71H88O10Si
There total 3 articles about C71H88O10Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C71H86O9Si;
With
dimethyl sulfide borane;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 3h;
DOI:10.1002/chem.201204303
- Guidance literature:
-
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/ja305864z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 1 h / 70 °C
2: borane-THF / tetrahydrofuran / 0.5 h / 20 °C
3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; borane-THF; dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; water; toluene;
DOI:10.1021/ja305864z