Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

Base Information

Chemical Name:Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane
CAS No.:77662-19-2
Molecular Formula:C₁₂H₁₃BrO₄S
Molecular Weight:335.187
Hs Code.:

Synonyms:Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

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Chemical Property of Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

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Technology Process of Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

There total 3 articles about Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 77662-18-1
syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

: 98-58-8
4-bromobenzenesulfonyl chloride

: 77662-19-2
Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

Guidance literature:: In pyridine;
DOI:10.1021/jo00330a027

Reference yield:

: 58101-60-3
methyl cyclopent-3-ene-1-carboxylate

: 77662-19-2
Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum deuteride / diethyl ether

2: m-chloroperbenzoic acid (85percent) / CH₂Cl₂

3: 75 percent / pyridine

With lithium aluminium deuteride; 3-chloro-benzenecarboperoxoic acid; In pyridine; diethyl ether; dichloromethane;
DOI:10.1021/jo00330a027

Reference yield:

: 77662-27-2
4-(Hydroxydideuteriomethyl)cyclopentene

: 77662-19-2
Brosylate Ester of syn-3-(Hydroxydideuteriomethyl)-6-oxabicyclo<3.1.0>hexane

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid (85percent) / CH₂Cl₂

2: 75 percent / pyridine

With 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane;
DOI:10.1021/jo00330a027